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Elements and Performance Criteria

  1. Plan work for shift
  2. Prepare sample racks for fusion
  3. Obtain acceptable buttons and prills
  4. Troubleshoot and correct common recovery failures
  5. Perform daily maintenance of assay equipment
  6. Maintain a safe work environment

Range Statement

This field allows for different work environments and conditions that may affect performance. Essential operating conditions that may be present (depending on the work situation, needs of the candidate, accessibility of the item, and local industry and regional contexts) are included.

Standards, codes, procedures and/or workplace requirements

Standards, codes, procedures and/or workplace requirements include the latest version of one or more of:

Australian and international standards covering the requirements for the competence of testing and calibration laboratories; laboratory safety; quality management and environmental management; analysis of specific ores and determination of gold; and labelling, storage, handling and transport of hazardous materials

national work health and safety (WHS) standards and codes of practice, national environmental protection measures, and national measurement regulations and guidelines

specific codes, guidelines and procedures, such as National Association of Testing Authorities (NATA) accreditation requirements and principles of good laboratory practice (GLP)

workplace documents, such as standard operating procedures (SOPs); quality and equipment manuals; maintenance schedules; material safety data sheets (MSDS) and safety procedures; material, production and product specifications; production and laboratory schedules; workplace recording and reporting procedures; and waste minimisation and safe disposal procedures

recovery methods and procedures for specific samples, sites and clients (labelling, preparation, storage, transport and disposal), and published preparation methods

Samples

Samples include, but are not limited to, one or more of:

solids, such as rocks, minerals, soils, sands and stream sediments

core and other drill samples (e.g. rotary air blast (RAB), reverse circulation (RC) and aircore)

slurries, powder concentrates and metallurgical solutions

dump samples and grab samples

Sequencing of pots in a rack

Sequencing of pots in a rack includes, but is not limited to, or more of:

addition of silver wire or silver nitrate (AGNO3) mix

addition of coloured salts (e.g. copper sulphate CuSO4)

Separation of collectors

Separation of collectors includes, but is not limited to, one or more of:

cupellation; digestion; and/or parting, annealing and weighing for a gravimetric finish

Hazards

Hazards include, but are not limited to, one or more of:

dust, silica, slag, glass shards and molten flux

chemicals, such as hydrofluoric acid, bromine, perchloric acid, aqua regia, cyanide, lead-based compounds, free-mercury and nickel compounds

noise and vibration

crushing, entanglement and cuts associated with moving machinery

manual handling of heavy loads, such as pots, racks and trolleys

heat exhaustion/stress and fatigue

Workplace safety procedures

Workplace safety procedures include, but are not limited to, one or more of:

ensuring access to service shut-off points, fire-extinguishers/fire hoses, safety shower/eye wash stations and first aid stations

recognising and observing hazard warnings and safety signs

labelling samples, reagents and hazardous materials

using direct extraction and fume hoods

providing guards for moving machinery parts

providing noise insulation

using PPE, such as dust masks, heat-resistant mittens, safety face shields with tinted visor, coats, ear muffs, safety boots, heat-reflective clothing and latex gloves for flux handling

following established manual handling procedures

regularly cleaning equipment and work areas

reporting abnormal emissions, discharges and airborne contaminants, such as noise, light, solids, liquids, water/wastewater, gasses, smoke, vapour, fumes, odour and particulates, to appropriate personnel

WHS and environmental management requirements

WHS and environmental management requirements include:

· complying with WHS and environmental management requirements at all times, which may be imposed through state/territory or federal legislation. These requirements must not be compromised at any time

· applying standard precautions relating to the potentially hazardous nature of samples


Performance Evidence

Evidence of competence in this unit must satisfy all of the requirements of the elements and performance criteria, and include demonstration of:

safely extracting precious metals from their host matrices in readiness for analysis on at least three (3) occasions

interpreting and following standard recovery methods

maintaining close attention to technical and safety requirements in a physically demanding, hazardous environment

recognising common sample preparation and cupellation problems and making standard adjustments to fluxes and firings

recognising non-acceptable characteristics of received and fused samples, buttons and prills

recognising indicators of poor recovery and applying established corrective actions

recognising the presence of highly oxidised ores, such as haematite or magnetite, and adjusting the charge weight and flux components to suit

accurately weighing samples and flux components

manually handling heavy and hot items of equipment safely

maintaining sequential control of samples through all recovery stages

keeping accurate and complete records, including:

pour sheets (date, time, client, pour number and preparation method)

number of pots, positions of sample, blank and check in rack

visual appearance of samples, buttons and prills

corrective actions for specific samples

planning work flow to ensure efficient sample throughput

minimising re-work, waste and environmental impacts and disposing of all waste responsibly

recognising hazards and using workplace safety procedures and safety equipment to work safely at all times.


Knowledge Evidence

Must provide evidence that demonstrates knowledge of:

procedures and/or standard methods for:

fusion of common mineral ore samples

cupellation of buttons

digestion/parting of prills

function, operation and maintenance of assay equipment used in job role

criteria for an 'acceptable' button, including:

one piece, mass >20 g and <50 g

malleable

separates cleanly from slag

free of undecomposed ore, matte and speiss

causes of contamination and losses, including:

poorly made cupels

base metals - copper (Cu), nickel (Ni), zinc (Zn) and bismuth (Bi)

arsenic (As), sulphur (S), antimony (Sb), selenium Se), tellurium (Te) and chromium (Cr)

scoria

sprouting

indicators of potential loss and the corrective action, including:

viscous slag (check furnace temperature, adjust flux and lower charge weight)

lead shotting – (adjust flux, lower charge weight to compensate for high oxides, silicates and chromites)

sulphides (adjust fusion time, adjust sample weight and/or flux)

matte, speiss (adjust sample weight and flux)

incomplete fusion (adjust sample weight and/or flux)

unacceptable button (adjust sample weight and/or flux)

inquartation (add three parts silver (Ag) to prill, wrap in lead foil and re-cupel)

workplace and legal traceability requirements

relevant hazards and control measures, operation and maintenance of safety equipment, work health and safety (WHS) and environment requirements.